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By Pei J., Zhang X.

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Presampling Steps . . . . . . . . . 1 Collection and storage of sample information . . . . . . . . . 2 Cleaning and evaluation of the instruments . . . . . . . . . . Collection and Storage of Blood . . . . Collection and Storage of Urine . . . . Collection and Storage of Tissues . . . . Microdialysis . . . . . . . . . . . 2 Antimony . . . . . . . . . . 3 Arsenic . . . . . . . . . . . 4 Cadmium . . . . . . . . .

All steps are carried out in clean laboratory conditions (class 100) except boiling for 8 h in the 1 : 1 mixture of concentrated acids. Other high purity items are cleaned in a similar way. , when the items are too small, they are boiled for an additional 6–8 h in Milli-Q water. 5 % HNO3 or 1 % EDTA with a final rinse in distilled water [6]. These procedures are undoubtedly too elaborate and too expensive for routine laboratory work in hospitals and are not necessary for all trace elements. Some authors even consider these procedures not necessary for short periods of storage (24 h).

4 Cadmium . . . . . . . . . . 5 Chromium . . . . . . . . . . 6 Cobalt . . . . . . . . . . . 23 24 24 24 27 29 30 31 8 33 33 34 34 9 35 10 35 11 36 INTRODUCTION Accuracy, quality assurance, quality control, repeatability, reproducibility, true value, validation, uncertainty of the measurement, . . and so many more concepts have become common language in any analytical laboratory. Indeed, these parameters should be carefully considered during an analysis but it is not a given fact that when these criteria are fulfilled the results will be perfect.

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