By Richard C. Larock
This long-awaited, greatly-expanded new version of a best-selling consultant deals an encyclopedic and systematic number of worthwhile artificial method, together with tens of hundreds of thousands of reactions and artificial variations. the 1st variation has been reviewed within the specialist journals as "clearly...the first selection for researchers looking info on artificial transformations." And as "useful to a person who needs to do natural synthesis, specially these whose concentration isn't strictly natural chemistry. It presents a...clear street map to the factitious literature and will be saved inside of effortless achieve of the chemist's desk."
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Chem. , 83, 4263, 1961. 44. , Reduktion tertiarer Phosphinoxyde zu tertiaren Phosphinen mit Silanen, Berichte, 97, 1988, 1964. 45. , Reduktion tertiarer Phosphinoxyde zu tertaren Phosphinen mit Trichlorosilan, Berichte, 98, 171, 1965. 46. , Perchloropolysilanes: novel reducing agents for phosphine oxides and other organic oxides, J. Am. Chem. , 91, 2788, 1969. 47. , The reaction of olefins with oxygen and phosphorus, J. Am. Chem. , 80, 4543, 1958. 48. , Chemical properties of the reaction product of cyclohexene with phosphorus and oxygen, J.
The supernatant layer was separated from the solid and concentrated to dryness to give the product α-hydroxy-p-methylbenzylphosphonous acid in 30% yield. 01 mol) in 57% aqueous HI (3 ml). The mixture was heated under reflux for 6 h. fm Page 22 Wednesday, November 19, 2003 10:56 AM to dryness under vacuum. The residue was dissolved in water that was then extracted with diethyl ether. The aqueous layer was concentrated to dryness, and the residue was recrystallized from 2-propanol/acetone to give the product benzylphosphonic acid in 25% yield.
J. Gen. , 67, 322, 1997. 23. , Phosphorylating power of red phosphorus toward aldehydes in basic and in acidic media, Eur. J. Org. , 861, 1999. 24. N. , Addition of dialkyl phosphites to unsaturated compounds. I. Addition of dialkyl phosphites to 2,2-dimethyl vinyl ketone, Zh. Obshch. Khim. , 21, 382, 1951. 25. , Regenerative role of red phosphorus in the couple HIaq/Pred, J. Organomet. , 529, 295, 1997. 26. , Alkylation of phosphorus iodides. V. Preparative method for dialkylphosphinic acids, Zh.