By L. J. Boucher, Karl Koeber, Mirjana Kotowski, Dieter Tille (auth.), Helga Demmer, Mirjana Kotowski, Edith Schleitzer-Rust, Dieter Tille (eds.)
Of system-number "Manganese", half B, which de- scribes the point Manganese, has been accomplished. additionally accomplished is an element C, describing the compounds, with 10 volumes. half A will current the historical past and occurence of manganese. quantity A 1 at the background has already been released, the opposite volumes facing occurence of manganese are in training. half D is dedicated to the coordination compounds. half D 1, D 2, D three, D four, D five and D 6 thereof are already on hand. the current quantity "Manganese D 7" maintains the outline of the coordination compounds. Complexes with nitriles, with nitro-hydrocarbons, and with ligands containing sulfur, selenium or tellurium are defined. a few of the coordination compounds containing sulfur are of analytical or organic curiosity. A formulation index lists the ligands and the empirical formulas.
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Extra resources for Coordination Compounds 7
0125 mol Mn" acetate. 0125 mol) was added slowly to the reaction solution. The red-brown product which precipitated during this second addition was obtained in a 50 to 60% yield . [(CeHshP(CH2CeHs)MMn"(C2HN02S2h1 was prepared by treating an Mn" salt with the sodium salt of ligand 1 and ahalide of the benzyltriphenylphosphonium cation. The X-ray powder patterns and IR spectrum (neither reported) were described as very similar to those of the corresponding CO", Ni", CU", Pd", and Pt" complexes.
J. Indian Chem. Soc. 42  483/5).  Paul, R. ; Pahil, S. S. (J. Indian Chem. Soc. 44  995/1000). GmeLin Handbook Mn Main Vol. 2 With Nitrobenzene, CaHsN02, or 1-Nitronaphthalene, Cl0 H7N0 2 [Mn"(CaHsN0:Jn][SbClah (n = 6, 3). The complex with n = 6 was obtained by stirring dehydrated manganese(lI) chloride with SbCls·CaHsN0 2 and nitrobenzene in the ratio 1:2:4 in nitromethane at room temperature. The pale yellow crystals precipitating at - 6°C from the solution were washed with sodium-dried pentane .
79 Ils at room temperature, determined by the Faraday technique. IR bands of the complex in Nujol or hexachlorobutadiene at 1708 and 1653 cm- 1 were assigned to v(G--o) vibrations, bands at 1455 and 1441 cm- 1 to v(G--CS 2) vibrations. Other bands in the 1300 to 800 cm- 1 range were not assigned. The IR spectrum is very similar to that of the Fe lV compound. In the UV-visible spectrum of the [Mn(C aH100 4S2hF- complex in CH 2Cl 2 , three bands were observed in the 26000 to 36000 cm- 1 range with f between 25000 and 59500 L· mol- 1 ·cm- 1 .