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By L. J. Boucher, Karl Koeber, Mirjana Kotowski, Dieter Tille (auth.), Helga Demmer, Mirjana Kotowski, Edith Schleitzer-Rust, Dieter Tille (eds.)

Of system-number "Manganese", half B, which de- scribes the point Manganese, has been accomplished. additionally accomplished is an element C, describing the compounds, with 10 volumes. half A will current the historical past and occurence of manganese. quantity A 1 at the background has already been released, the opposite volumes facing occurence of manganese are in training. half D is dedicated to the coordination compounds. half D 1, D 2, D three, D four, D five and D 6 thereof are already on hand. the current quantity "Manganese D 7" maintains the outline of the coordination compounds. Complexes with nitriles, with nitro-hydrocarbons, and with ligands containing sulfur, selenium or tellurium are defined. a few of the coordination compounds containing sulfur are of analytical or organic curiosity. A formulation index lists the ligands and the empirical formulas.

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Extra resources for Coordination Compounds 7

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0125 mol Mn" acetate. 0125 mol) was added slowly to the reaction solution. The red-brown product which precipitated during this second addition was obtained in a 50 to 60% yield [3]. [(CeHshP(CH2CeHs)MMn"(C2HN02S2h1 was prepared by treating an Mn" salt with the sodium salt of ligand 1 and ahalide of the benzyltriphenylphosphonium cation. The X-ray powder patterns and IR spectrum (neither reported) were described as very similar to those of the corresponding CO", Ni", CU", Pd", and Pt" complexes.

J. Indian Chem. Soc. 42 [1965] 483/5). [11] Paul, R. ; Pahil, S. S. (J. Indian Chem. Soc. 44 [1967] 995/1000). GmeLin Handbook Mn Main Vol. 2 With Nitrobenzene, CaHsN02, or 1-Nitronaphthalene, Cl0 H7N0 2 [Mn"(CaHsN0:Jn][SbClah (n = 6, 3). The complex with n = 6 was obtained by stirring dehydrated manganese(lI) chloride with SbCls·CaHsN0 2 and nitrobenzene in the ratio 1:2:4 in nitromethane at room temperature. The pale yellow crystals precipitating at - 6°C from the solution were washed with sodium-dried pentane [1].

79 Ils at room temperature, determined by the Faraday technique. IR bands of the complex in Nujol or hexachlorobutadiene at 1708 and 1653 cm- 1 were assigned to v(G--o) vibrations, bands at 1455 and 1441 cm- 1 to v(G--CS 2) vibrations. Other bands in the 1300 to 800 cm- 1 range were not assigned. The IR spectrum is very similar to that of the Fe lV compound. In the UV-visible spectrum of the [Mn(C aH100 4S2hF- complex in CH 2Cl 2 , three bands were observed in the 26000 to 36000 cm- 1 range with f between 25000 and 59500 L· mol- 1 ·cm- 1 .

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