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H6bel, M. Arch, Exptl. Pathol. Pharmakol. ~, 20. , Hbbel, M,, and Weege, C. 21. Cvoric, J. 22. Anghileri, L. J. 23. Taurog, A. 24. Schwane, R. A, and Kowkabany, G. N. 25. J. Chromatog. ~ 527 (1961). Z. Physiol. Chem. ~, 135 (1962). 349 (1969). Int. J. Appl, Radiat. Isotop. ~, Endocrinology& 759 (1957). 427 (1963). 581 (1963). Anal. Chem. ~, 1660 (1963). , Care, R. , and Rad~cella, R. Chem. —12, No. 2, 547 (1972). 26. Arino, H. and Kramer, H. H. Nucl. APP1. ~, 356 (1968). 27. Heydorn, K. J. Radioanal.

1241 by the reaction: . 4% 121Sb) beam energy antimony have been used as targets of 30 MeV was employed (313, for bombardment of the en- riched target(301); the beam energy for the natural antimony target was not given(313). Carrier-free 124I was separated from the natural antimony by dissolving target (along with the copper sulfuric acid, and distilling The isotonically wrapped dized were dissolved to a mixture of the oxyanions enriched on which it was soldered) the iodine, antimony in hydrochloric and adsorbing and the aluminum acid.

A novel gas-chromatographicprocedure for the rapid separation of fission iodine (or bromine) from the other fission-producedelements has been reported (97). The method is based on the fotmation of methyl iodide when uranium is irradiated in an atmosphere of methane. A thin uniform layer of “Krylon’’-lacquered uranium dioxide (natural uranium or enriched uranium-235) was deposited on an aluminum sheet and the sheet was placed in a plastic irradiation vial which was then filled with methane, closed, and placed in an irradiation rabbit.

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